in ethanol prepn. by refluxing ZnO with excess of carboxylic acid in EtOH for about2 h; cooled; ppt. filtered off; washed (EtOH) repeatedly; collected; kept over silica gel in vac. desiccator; elem. anal.;
参考文献
Taylor, Richard A.; Ellis, Henry A.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 1 p. 99 - 107
hydrogen fluoride bei der anodischen Fluorierung unter Verwendung einer Nickel-Anode und Behandlung des erhaltenen Pentadecafluoroctanoylfluorids mit Wasser;
参考文献
Kauck; Diesslin
Industrial and Engineering Chemistry, 1951 , vol. 43, p. 2332
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Minnesota Mining and Mfg.Co.
Patent: DE836796 , 1951 ;
DRP/DRBP Org.Chem.