in tetrahydrofuran; diethyl ether T=-90 - -85°C; 30 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
Rh(I)Cl(CO)(PMe3)2 P=760 Torr; 5 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
diethyl ether Darst. Reinigung durch Ueberfuehrung in 1.2-Dibrom-nonan und Zerlegung des Dibromids mit verkupfertem Zink in 90prozentigem Aethanol in der Waerme;