反应条件
1.1: tetrahydrofuran 2.1: Novozyme® 435 / hexane / 2 h / 32 °C / |Inert atmosphere; |Enzymatic reaction 3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C 4.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / |Inert atmosphere 4.2: -78 - 20 °C / |Inert atmosphere 5.1: Jone's reagent / diethyl ether / 5 h / 0 - 20 °C 6.1: hexane; tetrahydrofuran / 0.5 h / 20 °C / |Inert atmosphere 7.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 0 - 20 °C 8.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / |Inert atmosphere 8.2: 0.33 h / -78 °C 9.1: titanium tetrachloride / dichloromethane / 10 h / -78 - 20 °C / |Inert atmosphere View Scheme
参考文献
Ferrarini, Renan S.; Dos Santos, Alcindo A.; Comasseto, Joao V.
Tetrahedron, 2012 , vol. 68, # 51 p. 10601 - 10610,10
Title/Abstract Full Text Show Details
Ferrarini, Renan S.; Dos Santos, Alcindo A.; Comasseto, Joao V.
Tetrahedron, 2012 , vol. 68, # 51 p. 10601 - 10610
