1: With 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
P=760.051 Torr; 0.75 h;
2: With tributylphosphine; di-tert-butylazodicarboxylate in acetonitrile
Mitsunobu reaction; Inert atmosphere;
参考文献
Peterson, Scott L.; Stucka, Sabrina M.; Dinsmore, Christopher J.
Organic Letters, 2010 , vol. 12, # 6 p. 1340 - 1343
1: With tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=-40°C; P=760.051 Torr; Electrochemical reaction;
2: With hydrogenchloride in water; N,N-dimethyl-formamide
Sommer et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 1609,1611
Journal of the American Chemical Society, 1957 , vol. 79, p. 2764,2768