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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
124040-95-5
合成路线
(共 8 条)
124040-95-5
→
反应条件
602-09-5
1,1'-联-2-萘酚
反应条件
potassium hydroxide in ethanol T=25°C; 24 h;
参考文献
Lin, Gialih; Chen, Show-Jane; Sun, Hwey-Lin
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 4 p. 459 - 466
124040-95-5
→
反应条件
100465-50-7
+
25501-32-0
(S)-(+)-1-茚醇
+
158529-97-6
+
602-09-5
1,1'-联-2-萘酚
反应条件
1-hydroxyindan in diethyl ether; benzene 48 h; Heatinglipase from porcine pancreas, bovine serum albumin;
参考文献
Lin, Gialih; Chen, Show-Jane; Sun, Hwey-Lin
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 4 p. 459 - 466
124040-95-5
→
反应条件
18531-94-7
R-1,1'-联-2-萘酚
+
18531-99-2
S-联萘酚
反应条件
Arthrobacter sp. lipase in aq. phosphate buffer; N,N-dimethyl-formamide T=25°C; pH=7; 24 h; Resolution of racemateEnzymatic reaction; Solvent; enantioselective reaction;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal Ali; Mahajan, Neha; Chaubey, Asha; Taneja, Subhash Chandra
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 101, p. 35 - 39
124040-95-5
→
反应条件
18531-94-7
R-1,1'-联-2-萘酚
反应条件
Candida antarctica lipase B; acetophenone; butan-1-ol in various solvent(s) T=60°C; 96 h;
参考文献
Aoyagi, Naoto; Ogawa, Naomi; Izumi, Taeko
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4797 - 4801
124040-95-5
→
反应条件
100465-50-7
+
25501-32-0
(S)-(+)-1-茚醇
+
158529-97-6
+
602-09-5
1,1'-联-2-萘酚
反应条件
1-hydroxyindan in diethyl ether; benzene 48 h; Heatinglipase from porcine pancreas, bovine serum albumin;
参考文献
Lin, Gialih; Chen, Show-Jane; Sun, Hwey-Lin
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 4 p. 459 - 466
124040-95-5
→
反应条件
18531-94-7
R-1,1'-联-2-萘酚
+
18531-99-2
S-联萘酚
反应条件
Arthrobacter sp. lipase in aq. phosphate buffer; N,N-dimethyl-formamide T=25°C; pH=7; 24 h; Resolution of racemateEnzymatic reaction; Solvent; enantioselective reaction;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal Ali; Mahajan, Neha; Chaubey, Asha; Taneja, Subhash Chandra
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 101, p. 35 - 39
124040-95-5
→
反应条件
反应条件
Arthrobacter sp. lipase in aq. phosphate buffer; dimethyl sulfoxide T=25°C; pH=7; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal Ali; Mahajan, Neha; Chaubey, Asha; Taneja, Subhash Chandra
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 101, p. 35 - 39
6351-10-6
1-羟基茚满
+
124040-95-5
→
反应条件
18531-99-2
S-联萘酚
+
158529-97-6
反应条件
porcine pancreatic lipase in diethyl ether; benzene Heatingbovine albumin (fraction V);
参考文献
Lin, Gialih; Liu, Shih-Huang; Chen, Show-Jane; Wu, Fang-Chen; Sun, Hwey-Lin
Tetrahedron Letters, 1993 , vol. 34, # 38 p. 6057 - 6058