4-硝基-2-苯基苯甲酸合成路线 （共 10 条）
反应条件
potassium permanganate
参考文献
Ohkanda, Junko; Lockman, Jeffrey W.; Yokoyama, Kohei; Gelb, Michael H.; Croft, Simon L.; Kendrick, Howard; Harrell, Maria Isabel; Feagin, Jean E.; Blaskovich, Michelle A.; Sebti, Said M.; Hamilton, Andrew D.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 6 p. 761 - 764
反应条件
1: 89 percent / Pd(OAc)2; K2CO3 2: 100 percent / KMnO4 View Scheme
参考文献
Augeri, David J.; O'Connor, Stephen J.; Janowick, Dave; Szczepankiewicz, Bruce; Sullivan, Gerry; Larsen, John; Kalvin, Douglas; Cohen, Jerry; Devine, Edward; Zhang, Haichao; Cherian, Sajeev; Saeed, Badr; Ng, Shi-Chung; Rosenberg, Saul
Journal of Medicinal Chemistry, 1998 , vol. 41, # 22 p. 4288 - 4300
反应条件
1: 88 percent / potassium carbonate hydrate; Pd(OAc)2 / acetone / 10 h / Heating 2: 85 percent / KMnO4 / pyridine; H2O / 5 h / Heating View Scheme
参考文献
Ohkanda, Junko; Lockman, Jeffrey W.; Yokoyama, Kohei; Gelb, Michael H.; Croft, Simon L.; Kendrick, Howard; Harrell, Maria Isabel; Feagin, Jean E.; Blaskovich, Michelle A.; Sebti, Said M.; Hamilton, Andrew D.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 6 p. 761 - 764
反应条件
potassium permanganate in acetone 4 h; Ambient temperature;
参考文献
Iihama, T.; Fu, J.-m.; Bourguignon, M.; Snieckus, V.
Synthesis, 1989 , # 3 p. 184 - 188
参考文献
Ray; Barrick
Journal of the American Chemical Society, 1948 , vol. 70, p. 1492
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Braker; Christiansen
Journal of the American Pharmaceutical Association (1912-1977), 1935 , vol. 24, p. 358,360
反应条件
1: AgNO3 / dioxane; H2O / 18 h / Ambient temperature 2: aq. KOH / dioxane / 20 h / Ambient temperature 3: 98 percent / aq. KMnO4 / acetone / 4 h / Ambient temperature View Scheme
参考文献
Iihama, T.; Fu, J.-m.; Bourguignon, M.; Snieckus, V.
Synthesis, 1989 , # 3 p. 184 - 188
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere 2: sodium hydroxide; water / tetrahydrofuran / 80 °C View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
1: 88 percent / polyphosphoric acid / 5 h / 160 °C 2: 14 percent / Et3SiH / trifluoroacetic acid / 48 h / Ambient temperature View Scheme
参考文献
Iihama, T.; Fu, J.-m.; Bourguignon, M.; Snieckus, V.
Synthesis, 1989 , # 3 p. 184 - 188
参考文献
Iihama, T.; Fu, J.-m.; Bourguignon, M.; Snieckus, V.
Synthesis, 1989 , # 3 p. 184 - 188
反应条件
1: 88 percent / polyphosphoric acid / 5 h / 160 °C
2: 73 percent / Et3SiH / trifluoroacetic acid / 48 h / Ambient temperature
View Scheme
参考文献
Iihama, T.; Fu, J.-m.; Bourguignon, M.; Snieckus, V.
Synthesis, 1989 , # 3 p. 184 - 188
