N-{(1Z,4Z)-4-[(苯磺酰基)亚氨基]-2,5-环己二烯-1-亚基}苯甲酰胺合成路线 (共 6 条)
反应条件
lead(IV) acetate in chloroform T=25°C; 12 h;
参考文献
Boger; Zarrinmayeh
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1379 - 1390
反应条件
1: 99 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h / 25 °C / 2585.7 Torr 2: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating 3: 79 percent / lead tetraacetate / CHCl3 / 12 h / 25 °C View Scheme
参考文献
Boger; Zarrinmayeh
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1379 - 1390
反应条件
1: 84 percent / pyridine / tetrahydrofuran / 8 h / Heating 2: 79 percent / lead tetraacetate / CHCl3 / 12 h / 25 °C View Scheme
参考文献
Boger; Zarrinmayeh
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1379 - 1390
反应条件
boron trifluoride diethyl etherate T=25°C; 8 h; also catalyzed by H2SO4;
参考文献
Journal of Organic Chemistry, , vol. 55, # 4 p. 1379 - 1390
反应条件
in diethyl ether
T=-20°C; 12 h;
参考文献
Boger; Zarrinmayeh
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1379 - 1390
反应条件
hydrogenchloride; water; acetic acid
参考文献
Adams; Colgrove
Journal of the American Chemical Society, 1954 , vol. 76, p. 3584,3585