in neat (no solvent) byproducts: Cl2; Cl2O6 added to SbCl5 at -180°C in Pyrex reactor, mixt. allowed to warm slowly to 10°C, gases removed periodically; unreacted SbCl5 pumped out, elem. anal.;
参考文献
Belin, C.H.; Chaabouni, M.; Pascal, J.L.; Potier, J.
Inorganic Chemistry, 1982 , vol. 21, p. 3557 - 3560
in neat (no solvent) byproducts: Cl2; Cl2O6 added to SbCl5 at -180°C in Pyrex reactor, mixt. allowed to warm slowly to 10°C, gases removed periodically; unreacted SbCl5 pumped out, elem. anal.;
参考文献
Belin, C.H.; Chaabouni, M.; Pascal, J.L.; Potier, J.
Inorganic Chemistry, 1982 , vol. 21, p. 3557 - 3560
