胆固醇-5Alpha,6Alpha-环氧化物合成路线 (共 40 条)
反应条件
Fe(III)TpCPP; dihydrogen peroxide in 2,2,4-trimethylpentane; water 12 h; other sterols, other iron(III) porphyrins; var. water/surfactant ratio and pH; oxidation in AOT reversed micelles; Product distribution;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 12 p. 837 - 843
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 47, p. 93
参考文献
Yakugaku Zasshi, , vol. 60, p. 334,338; engl. Ref. S. 125
Chem.Abstr., , p. 7294
反应条件
1: 91 percent / pyridine / diethyl ether 2: 48percent aq. hydrobromic acid / CHCl3 / 0.25 h 3: 60 percent / N,N-dimethylaniline / H2O / 44 h / Heating 4: 1 percent / tributylstannane, AIBN / benzene / 0.83 h / 80 °C View Scheme
参考文献
Beckwith, Athelstan L. J.; Duggan, Peter J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 10 p. 1777 - 1783
反应条件
in acetic acid 8 h; Heating;
参考文献
Journal of the Indian Chemical Society, , vol. 65, p. 292 - 293
反应条件
aluminium(III) iodide in acetonitrile; benzene 0.0833333 h;
参考文献
Sarmah, Parijat; Barua, Nabin C
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5815 - 5816
反应条件
oxygen; platinum in water; acetone T=80°C; P=760 Torr; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 3023 - 3025
反应条件
mercaptoacetic acid; N,N-dimethyl-formamide; lithium bromide T=60 - 80°C; 12 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 7 p. 700 - 701
反应条件
mercaptoacetic acid; lithium bromide T=60 - 80°C; 12 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 7 p. 700 - 701
参考文献
Zhurnal Obshchei Khimii, , vol. 9, p. 1690
Chem. Zentralbl., , vol. 111, # I p. 1995
Journal of the American Chemical Society, , vol. 74, p. 5362