3,3',5,5'-四溴-2,2'-联噻吩合成路线 (共 18 条)
参考文献
Hwang, In-Ho; Lee, Min-Jeong
Patent: US2010/240910 A1, 2010 ;
Location in patent: Page/Page column 13-15 ;
反应条件
N-bromosuccinmide; acetic acid in chloroform T=20 - 50°C; 20 h;
参考文献
Pozzi, Gianluca; Orlandi, Simonetta; Cavazzini, Marco; Minudri, Daniela; Macor, Lorena; Otero, Luis; Fungo, Fernando
Organic Letters, 2013 , vol. 15, # 18 p. 4642 - 4645
反应条件
N-bromosuccinmide in chloroform; acetic acid 5 h; Heating;
参考文献
Yui, Koji; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 5 p. 1539 - 1546
反应条件
N-bromosuccinmide in chloroform; acetic acid 72 h; Heating;
参考文献
Dahlmann, Uwe; Neidlein, Richard
Helvetica Chimica Acta, 1996 , vol. 79, # 3 p. 755 - 766
反应条件
copper dichloride in diethyl ether T=-78°C; 2 h;
参考文献
Dahlmann, Uwe; Neidlein, Richard
Helvetica Chimica Acta, 1996 , vol. 79, # 3 p. 755 - 766
反应条件
potassium fluoride; bis(benzonitrile)palladium(II) dichloride; silver nitrate in dimethyl sulfoxide T=20°C; 24 h;
参考文献
Takahashi, Masabumi; Masui, Kentaro; Sekiguchi, Hiroki; Kobayashi, Nobuhiko; Mori, Atsunori; Funahashi, Masahiro; Tamaoki, Nobuyuki
Journal of the American Chemical Society, 2006 , vol. 128, # 33 p. 10930 - 10933
参考文献
Justus Liebigs Annalen der Chemie, , vol. 527, p. 272,276
反应条件
hydrogenchloride; water; acetic acid; zinc in ethanol 2 h; Reflux;
参考文献
Letizia, Joseph A.; Cronin, Scott; Ortiz, Rocio Ponce; Facchetti, Antonio; Ratner, Mark A.; Marks, Tobin J.
Chemistry - A European Journal, 2010 , vol. 16, # 6 p. 1911 - 1928
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille coupling; 24 h; RefluxInert atmosphere;
参考文献
Piron, Flavia; Leriche, Philippe; Grosu, Ion; Roncali, Jean
Journal of Materials Chemistry, 2010 , vol. 20, # 45 p. 10260 - 10268
反应条件
1.1: 90 percent / zinc; HCl / ethanol; H2O; acetic acid / 2 h / Heating 2.1: n-BuLi / hexane; tetrahydrofuran / 1.5 h / -78 °C 2.2: 68 percent / hexane; tetrahydrofuran / -78 - 20 °C 3.1: 91 percent / NBS / dimethylformamide / 0.17 h / 20 °C View Scheme
参考文献
Kim, Ki-Won; Na, Hyungjun; So, Won-Wook; Yoon, Sung Cheol; Shin, Won Suk
Journal of Nanoscience and Nanotechnology, 2012 , vol. 12, # 5 p. 4279 - 4283