4-(二乙基磷甲基)苯甲醛合成路线 （共 11 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 2 h;
参考文献
Loewe, Robert S.; Ambroise, Arounaguiry; Muthukumaran, Kannan; Padmaja, Kisari; Lysenko, Andrey B.; Mathur, Guru; Li, Qiliang; Bocian, David F.; Misra, Veena; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2004 , vol. 69, # 5 p. 1453 - 1460
反应条件
sodium hydrogencarbonate in dimethyl sulfoxide T=130°C; 4 h;
参考文献
Mayer, Cedric R.; Herve, Maryline; Lavanant, Helene; Secheresse, Francis
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7805 - 7807
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in acetic acid T=100°C; 3 h;
参考文献
Madathil, Rethi; Parkesh, Raman; Draper, Sylvia M.
Tetrahedron Letters, 2006 , vol. 47, # 16 p. 2731 - 2734
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
G. D. Searle and Co.
Patent: US4918064 A1, 1990 ;
参考文献
Wang, Xiang-Zhu; Burke Jr., Terrence R.
Synlett, 2004 , # 3 p. 469 - 472
反应条件
1: DIBALH 2: 86 percent / 4 h / Heating View Scheme
参考文献
Wang, Xiang-Zhu; Burke Jr., Terrence R.
Synlett, 2004 , # 3 p. 469 - 472
反应条件
1: 77 percent / toluene / 18 h / Heating 2: BH3 / tetrahydrofuran / 4 h / 20 °C 3: 6.54 g / PCC / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Loewe, Robert S.; Ambroise, Arounaguiry; Muthukumaran, Kannan; Padmaja, Kisari; Lysenko, Andrey B.; Mathur, Guru; Li, Qiliang; Bocian, David F.; Misra, Veena; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2004 , vol. 69, # 5 p. 1453 - 1460
反应条件
1: BH3 / tetrahydrofuran / 4 h / 20 °C 2: 6.54 g / PCC / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Loewe, Robert S.; Ambroise, Arounaguiry; Muthukumaran, Kannan; Padmaja, Kisari; Lysenko, Andrey B.; Mathur, Guru; Li, Qiliang; Bocian, David F.; Misra, Veena; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2004 , vol. 69, # 5 p. 1453 - 1460
反应条件
1: 50 percent / 3 h / 120 °C 2: 90 percent / hexamethylene tetraamine / acetic acid / 3 h / 100 °C View Scheme
参考文献
Madathil, Rethi; Parkesh, Raman; Draper, Sylvia M.
Tetrahedron Letters, 2006 , vol. 47, # 16 p. 2731 - 2734
反应条件
1: 76 percent / N-bromosuccinimide; dibenzoylperoxide / CCl4 / 3 h / Irradiation; heating 2: 88 percent / NaHCO3 / dimethylsulfoxide / 4 h / 130 °C View Scheme
参考文献
Mayer, Cedric R.; Herve, Maryline; Lavanant, Helene; Secheresse, Francis
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7805 - 7807
