5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile 1.) 0 deg C, 5 min, 2.) room temperature, overnight;
参考文献
Anulewicz; Krygowski; Jagodzinski
Polish Journal of Chemistry, 1998 , vol. 72, # 2 p. 439 - 448
反应条件
in ethanol 3 h; Heating;
参考文献
Rao, T. Vedagiriswani; Ravishankar; Baskaran; Trivedi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 6 p. 546 - 551
反应条件
(COBr)2; N,N-dimethyl-formamide in dichloromethane 0 deg C, 5 min, then to room temp., 30 min;
参考文献
Tetrahedron Letters, , vol. 30, # 29 p. 3753 - 3756
反应条件
1: 43 percent / acetic acid / 3 h / Heating 2: 49 percent / hydrazine hydrate / ethanol / 1 h / Heating View Scheme
参考文献
Erian, Ayman W.; Sherif, Sherif M.; Mohamed, Nadia R.
Synthetic Communications, 2003 , vol. 33, # 9 p. 1563 - 1573
反应条件
NaHSO4 on SiO2 solid support 0.133333 h; Microwave irradiationNeat (no solvent);
参考文献
Journal of the Korean Chemical Society, , vol. 54, # 6 p. 723 - 726
反应条件
in acetic acid T=110°C; Condensation; 1.5 h;
参考文献
Upton, Mathew; Jaeda, Moussa I.; Upton, Christopher
Journal of Pharmacy and Pharmacology, 1998 , vol. 50, # 5 p. 475 - 482
反应条件
1: aqueous KOH 2: platinum; methanol / Hydrogenation View Scheme
参考文献
Nickl
Chemische Berichte, 1958 , vol. 91, p. 553,563
反应条件
[BsMIm][HSO4] T=120°C; 0.5 h; Catalytic behavior; ConcentrationTemperatureSolvent;
参考文献
Song, Shihua; Deng, Xiang; Guan, Zhi; He, Yanhong
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 7 p. 717 - 724
反应条件
[N-butylthiazolium][Br]; hydrazine hydrate T=25 - 30°C; 0.05 h; Ultrasonic irradiation;
参考文献
Shekouhy, Mohsen; Hasaninejad, Alireza
Ultrasonics Sonochemistry, 2012 , vol. 19, # 2 p. 307 - 313
反应条件
phosphorous pentoxide T=80°C; 0.666667 h; Neat (no solvent);
参考文献
Shukla, Gaurav; Verma, Rajiv K.; Verma, Girijesh K.; Singh, Maya Shankar
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7195 - 7198