5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
反应条件
in dichloromethane
T=20 - 80°C; 4 h; Sealed tube;
参考文献
Lasri, Jamal
Letters in Organic Chemistry, 2013 , vol. 10, # 7 p. 482 - 489
反应条件
in N,N-dimethyl-formamide
1 h; Reflux; regioselective reaction;
参考文献
Lipson; Svetlichnaya; Shirobokov; Musatov; Shishkin; Shishkina
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 2 p. 273 - 277
反应条件
piperidine in isopropyl alcohol
0.333333 h; Heating;
参考文献
Pyrko
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 635 - 645
反应条件
L-proline in methanol
T=20°C; 12 h; Reagent/catalystSolvent;
参考文献
Ganguly, Nemai C.; Roy, Sushmita; Mondal, Pallab; Saha, Rajat
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7067 - 7071
反应条件
6-amino-quinoline in butan-1-ol
Heating;
参考文献
Gusak; Tereshko; Kozlov
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 10 p. 1495 - 1502
反应条件
1: TiCl4 / Irradiation
2: TiCl4 / Irradiation
3: aq. HCl / methanol / Heating
View Scheme
参考文献
Sato,T. et al.
Bulletin of the Chemical Society of Japan, 1977 , vol. 50, p. 2714 - 2730
反应条件
toluene
T=170 - 180°C;
参考文献
Hoffmann-La Roche
Patent: DE614195 , 1934 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 615
反应条件
1.1: potassium hydroxide / water; ethanol / 0.25 h
1.2: 12 h / 20 °C
2.1: acetic acid; ammonium acetate / 3 h / 140 °C
View Scheme
参考文献
Gonzalez-Chavez, Rodolfo; Martinez, Roberto; Torre-Bouscoulet, Maria Eugenia; Gallo, Marco; Gonzalez-Chavez, Marco Martin
Chemical and Pharmaceutical Bulletin, 2014 , vol. 62, # 1 p. 16 - 24
反应条件
pyridine in chloroform
参考文献
Chevron Research Company
Patent: US4440566 A1, 1984 ;
Title/Abstract Full Text Show Details
Chevron Research Company
Patent: US32489 E1, 1987 ;
反应条件
potassium carbonate in ethanol
T=70°C; 4 h;
参考文献
Krief; Surleraux; Frauenrath
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6157 - 6160
