5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
参考文献
Suomen Kemistilehti B, , vol. 8, p. 32
Chem. Zentralbl., , vol. 107, # I p. 2076
参考文献
Justus Liebigs Annalen der Chemie, , vol. 294, p. 335 Anm.5
参考文献
Chemische Berichte, , vol. 34, p. 1955
反应条件
sodium hydride in N,N-dimethyl-formamide 24 h;
参考文献
Bilinski, Vanda; Dreiding, Andre S.
Helvetica Chimica Acta, 1985 , vol. 68, p. 2140 - 2147
反应条件
1: 82.5 percent / p-CH3C6H4SO3H / benzene / Heating 2: 91 percent / LiAlH4 3: 91 percent / LiAlH4 4: 81 percent / propionic acid / 36 h / 138 °C View Scheme
参考文献
Wawrzenczyk, Czeslaw; Lochynski, Stanislaw
Monatshefte fuer Chemie, 1985 , vol. 116, p. 99 - 110
反应条件
silica-supported LiHSO4 T=80°C; 0.1 h; Neat (no solvent);
参考文献
Journal of the Iranian Chemical Society, , vol. 7, # 1 p. 69 - 76
反应条件
1: 82.5 percent / p-CH3C6H4SO3H / benzene / Heating 2: 91 percent / LiAlH4 3: 91 percent / LiAlH4 4: 81 percent / propionic acid / 36 h / 138 °C 5: LiAlH4 6: 74 percent / C5H5N View Scheme
参考文献
Wawrzenczyk, Czeslaw; Lochynski, Stanislaw
Monatshefte fuer Chemie, 1985 , vol. 116, p. 99 - 110
反应条件
1: 1.) phosphorous oxychloride; 2.) sodium 2: 70 percent / Jones reagent / acetone / 1.) 0 deg.C, 2 h.; 2.) 2 h. room temp 3: 93 percent / diethyl ether / 0.5 h / Heating 4: 1.) phosphorous oxychloride; 2.) H2 / 2.) PtO2 / 1.) 4 h. room temp; 1.5 h, reflux, pyridine; 2.) 3 h room temp, acetic acid, 26 psi. View Scheme
参考文献
Forrest, T. P.; Thiel, J.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2870 - 2875
反应条件
sodium acetate; acetic acid; zinc 1 h; Heating; Yield given;
参考文献
Nenitzescu; Scortzeanu
Bulet. Soc. chim. Romania, vol. 10, p. 134
Chem. Zentralbl., 1929 , vol. 100, # I p. 2185
反应条件
in benzene T=20°C; 2.5 h;
参考文献
Levchenko, E. S.; Budnik, L. V.; Kalinin, V. N.; Kisilenko, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 12 p. 2249 - 2251
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2549 - 2552
