2-氯-1.3-丁二烯合成路线 （共 128 条）
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane
T=-5 - 0°C; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane
T=-5 - 0°C; Further byproducts given. Yields of byproduct given;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane
T=-5 - 0°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
反应条件
tert-butyl-pyrocatechol; chlorine in tetrachloromethane
T=-5 - 0°C; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mkryan, G. M.; Airapetyan, R. Kh.; Mkryan, G. G.; Kaplanyan, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 1242 - 1247
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1387 - 1393
反应条件
Chlorieren bei tiefen Temperaturen;
参考文献
du Pont de Nemours and Co.
Patent: US1965369 , 1932 ;
Full Text Show Details
Petrow
Zhurnal Obshchei Khimii, 1943 , vol. 13, p. 111
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1050
Chem.Abstr., 1944 , p. 330,1950 1003
参考文献
Carothers; Berchet
Journal of the American Chemical Society, 1933 , vol. 55, p. 1629
Full Text Show Details
Petrow
Zhurnal Obshchei Khimii, 1943 , vol. 13, p. 111
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1050
Chem.Abstr., 1944 , p. 330,1950 1003
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran
T=0°C; Negishi coupling; 2 h;
参考文献
Bradford, Tanya A.; Payne, Alan D.; Willis, Anthony C.; Paddon-Row, Michael N.; Sherburn, Michael S.
Organic Letters, 2007 , vol. 9, # 23 p. 4861 - 4864
反应条件
bis (3-tert-butyl-4-hydroxy-5-methyl phenyl)-sulfide in toluene
T=50°C; 16 h; Further byproducts given;
参考文献
Klaerner, Frank-Gerrit; Krawczyk, Bernd; Ruster, Volker; Deiters, Ulrich K.
Journal of the American Chemical Society, 1994 , vol. 116, # 17 p. 7646 - 7657
反应条件
2,4,6-trinitro-phenol
T=80°C;
参考文献
Stewart,C.A.
Journal of the American Chemical Society, 1971 , vol. 93, # 19 p. 4815 - 4821
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform-d1; water-d2
T=20°C; 140 h; Product distribution;
参考文献
Cottrell; Golding; Munter; Watson
Chemical Research in Toxicology, 2001 , vol. 14, # 11 p. 1552 - 1562
