反应条件
1: 2-(2-pyridyl)-5-methylpyridine With N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=85°C; 8 h; Inert atmosphere; 2: sodium acetate With acetic acid 36 h; Reflux; 3: With hydrogenchloride in water 51 h; Reflux; Overall yield = 144 mg;
参考文献
Nakamura, Takashi; Ube, Hitoshi; Shiro, Motoo; Shionoya, Mitsuhiko
Angewandte Chemie - International Edition, 2013 , vol. 52, # 2 p. 720 - 723
Angew. Chem., 2013 , vol. 125, # 2 p. 748 - 751,4
