反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / |Schlenk technique; |Inert atmosphere 1.2: |Schlenk technique; |Inert atmosphere 2.1: potassium tert-butylate / tetrahydrofuran / 0 °C / |Schlenk technique; |Inert atmosphere 3.1: (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium / toluene / 1 h / 100 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Matsuda, Takanori; Sato, Shinya
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3329 - 3335
