反应条件
FeCl3 in tetrahydrofuran
under Ar, in flask with Mg chips added anhyd. FeCl3, cycloheptatriene, THF, and, over 3-h period to allow warming stirred mixt., soln. of Ti complex in THF, mixt. stirred at room temp. for 12 h; volatile products evapd. under vac., residue sublimed at 130°C (E-2 mmHg), solid washed with hexane, dried under vac.;
参考文献
Demerseman, Bernard; Dixneuf, Pierre H.; Douglade, Jacques; Mercier, Rene
Inorganic Chemistry, 1982 , vol. 21, p. 3942 - 3947
