反应条件
in dichloromethane exclusion of air, moisture, light; dropwise addn. of S2Cl2 in CH2Cl2 to Ti-complex in CH2Cl2 (0°C); vol. redn. (vac.), chromy. (Bio-Beads, CH2Cl2, >=15°C in the dark), evapn.; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 388, # 1+2 p. 89 - 94