in diethyl ether; toluene
byproducts: LiCl; (N2); standard Schlenk technique; soln. of MeLi in ether was added to suspn. of Ti complex in toluene; mixt. was stirred at 0°C for 3 h; filtered; volatiles removed (vac.); residue redissolved in toluene; NMR monitoring;
参考文献
Bryliakov, Konstantin P.; Talsi, Evgenii P.; Bochmann, Manfred
Organometallics, 2004 , vol. 23, # 1 p. 149 - 152
triphenylphosphine in toluene
Irradiation (UV/VIS); sample sealed under vac. in silica tubes, photolyzed with light from 500 W high pressure Hg arc at -80 to -6°C; not isolated; detected by ESR;
参考文献
Brindley, Peter B.; Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 247 - 256
in tetrahydrofuran; toluene
Irradiation (UV/VIS); samples sealed under vac. in silica tubes, photolyzed with light from 500 W high pressure Hg arc at -14 or -34°C; not isolated; detected by ESR;
参考文献
Brindley, Peter B.; Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 247 - 256
in toluene
Irradiation (UV/VIS); sample sealed under vac. in silica tubes, photolyzed with light from 500 W high pressure Hg arc at -80 to -6°C; not isolated; detected by ESR;
参考文献
Brindley, Peter B.; Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 247 - 256
in toluene
Irradiation (UV/VIS); sample sealed under vac. in silica tubes, photolyzed with light from 500 W high pressure Hg arc at -33°C; not isolated; detected by ESR;
参考文献
Brindley, Peter B.; Davies, Alwyn G.; Hawari, Jalal A.-A.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 247 - 256
