water in water oxidn. in air; KI addn. to aq. soln.; filtering; washing with water, then with ether; vac. drying at room temp.; purity controlled IR, UV spect. and microanal.;
参考文献
Li, T. T.- T.; Brubaker, C.H.
Journal of Organometallic Chemistry, 1981 , vol. 216, # 2 p. 223 - 234
aluminium trichloride; air; sulfur dioxide in ethanol; ammonia; acetic acid react. of (C6H6)2Cr and AlCl3;decompn. with NH3/ice;oxidn. with air;pptg. with KI3 in acetic acid;adding SO2 in ethanol to the formed mixture;
aluminium trichloride; I2; water react. of (C6H6)2Cr with (C6H5C6H5)2Cr in presence of AlCl3 at 120 °C; hydrolysis with NH3/ice; oxidn. with air; filtration; addn. of KI3/HO2CCH3; treating with SO2/ethanol;;
参考文献
Hein, F.; Kartte, K.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1960 , vol. 307, p. 22 - 37
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Gmelin Handbook: Cr: Org.Verb., 1.6.2.1.1.1.2, page 316 - 318
