in N,N-dimethyl-formamide Electrolysis; cathode - Pt foil (1X1 cm), anode - sheet of Cu (5X5X0.2 cm) upon which thick layer of Cu freshly deposited electrochemically; soln. of alcohol in DMF and (Bu4N)Cl stirred in electrolysis cell, current of 20 mA (potential 6 V) passed through cell (6 h); filtered, washed with Et2O, dried in vac.; elem. anal.;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 16, p. 1217 - 1224
in nitric acid aq. HNO3; Dissolving copper metal in a mixt. of HNO3 and distd. water followed twice by evapn. to near dryness and addn. of a mixt. of acetic acid and distd. water.; Not isolated.;
参考文献
DeSisto, W.; Sosnowski, M.; Smith, F.; Deluca, J.; Kershaw, R.; et al.
Materials Research Bulletin, 1989 , vol. 24, p. 753 - 760
Koontz, D. E.; Nicholson, D. G.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1936 - 1937
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Gmelin Handbook: Cu: MVol.A2, 213, page 1270 - 1273
Rochow synthesis, heating with a mixture of 60percent Ge and 40 percent Cu at 650°C;;
参考文献
Weidenbruch, M.; Wessal, N.
Chemische Berichte, 1972 , vol. 105, p. 173 - 187
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Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169
