反应条件
HCl in diethyl ether
addn. during 20 min at 20°C, mixt. was stirred for further 40 min; volatiles were removed in vac., 1H NMR showed two component in a solid,latter product was isolated by fractional recrystn.;
参考文献
Jeffery, John; Lappert, Michael F.; Luong-Thi, N. Tuyet; Webb, Maurice; Atwood, Jerry L.; Hunter, William E.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 1593 - 1605
