2-乙炔基-6-甲氧基萘合成路线 （共 12 条）
反应条件
methanol; potassium carbonate in tetrahydrofuran 2 h;
参考文献
Arakawa, Yuki; Nakajima, Shunpei; Kang, Sungmin; Shigeta, Masayuki; Konishi, Gen-Ichi; Watanabe, Junji
Journal of Materials Chemistry, 2012 , vol. 22, # 28 p. 13908 - 13910
反应条件
sodium hydroxide in toluene 17 h; Heating;
参考文献
Hiyama; Wakasa; Ueda; Kusumoto
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 2 p. 640 - 642
反应条件
1: Pd(PPh3)4; PPh3 / CuBr2; LiBr / various solvent(s); tetrahydrofuran / 2 h / 90 °C 2: 83 percent / KOH / various solvent(s) / 0.05 h / 150 °C / 30 Torr View Scheme
参考文献
Hiyama; Wakasa; Ueda; Kusumoto
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 2 p. 640 - 642
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; oxygen in diethylamine; acetonitrile T=120°C; Sonogashira coupling; 0.25 h; Microwave irradiation;
参考文献
Gising, Johan; Nilsson, Mikael T.; Odell, Luke R.; Yahiaoui, Samir; Lindh, Martin; Iyer, Harini; Sinha, Achyut M.; Srinivasa, Bachally R.; Larhed, Mats; Mowbray, Sherry L.; Karlen, Anders
Journal of Medicinal Chemistry, 2012 , vol. 55, # 6 p. 2894 - 2898
反应条件
1: potassium carbonate / acetonitrile / 3 h / Reflux 2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine; triphenylphosphine / tetrahydrofuran / 15 h / 20 °C 3: methanol; potassium carbonate / tetrahydrofuran / 2 h View Scheme
参考文献
Wong, Man Shing; Nicoud, Jean-Francois
Journal of the Chemical Society, Chemical Communications, 1994 , # 3 p. 249 - 250
反应条件
1: POCl3 / 20 °C 2: NaOH / dioxane; H2O / 20 °C View Scheme
参考文献
Kotha; Tafesh; Davenport; Ortiz
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 12 p. 1166 - 1169
反应条件
water; silver trifluoromethanesulfonate 5.5 h; Heating;
参考文献
Das, Rima; Chakraborty, Debashis
Applied Organometallic Chemistry, 2012 , vol. 26, # 12 p. 722 - 726
反应条件
hydrogen; platinum nanoparticles in methanol T=90°C; P=10343.2 Torr; 4.5 h; Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 13 p. 2145 - 2150
反应条件
hydrogen; N1-(2-Amino-ethyl)-ethane-1,2-diamine in methanol T=25°C; 6 h;
参考文献
Yabe, Yuki; Yamada, Tsuyoshi; Nagata, Saori; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1264 - 1268
反应条件
potassium hydroxide; polyethylene glycol (PEG-400); potassium cyanide; nickel cyanide; cobalt(II) chloride in toluene T=90°C; P=760 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 32, # 15 p. 1769 - 1770
