6,7-二甲氧基-1-乙烯基-1,2,3,4-四氢-异喹啉合成路线 （共 3 条）
反应条件
(2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one in acetonitrile T=20°C; 32 h;
参考文献
Kinderman, Sape S.; Wekking, Monique M. T.; Van Maarseveen, Jan H.; Schoemaker, Hans E.; Hiemstra, Henk; Rutjes, Floris P. J. T.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5519 - 5527
反应条件
1: 96 percent / Et3N / CH2Cl2 / 6 h / 20 °C 2: 42 percent / Et3N / Pd(OAc)2 / acetonitrile / 6 h / 20 °C 3: 74 percent / Sn(OTf)2 / CH2Cl2 / 0 °C 4: 83 percent / PhSK / acetonitrile / 32 h / 20 °C View Scheme
参考文献
Kinderman, Sape S.; Wekking, Monique M. T.; Van Maarseveen, Jan H.; Schoemaker, Hans E.; Hiemstra, Henk; Rutjes, Floris P. J. T.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5519 - 5527
反应条件
in tetrahydrofuran 60 h; Ambient temperature; Further byproducts given;
参考文献
Grigg, R.; Gunaratne, H. Q. Nimal; Henderson, Deirdre; Sridharan, Visuvanathar
Tetrahedron, 1990 , vol. 46, # 5 p. 1599 - 1610
