1-甲氧基-4-[4-(4-甲氧基苯基)己烷-3-基]苯合成路线 (共 35 条)
反应条件
hydrogenchloride; palladium on activated charcoal T=60°C; Hydrogenation;
参考文献
Merck,E.
Patent: DE735867 , 1941 ;
DRP/DRBP Org.Chem.
反应条件
T=210°C; P=194910 Torr; Hydrogenation;
参考文献
Hoehn; Ungnade
Journal of the American Chemical Society, 1945 , vol. 67, p. 1617
反应条件
n-butyllithium; titanium(III) chloride; triethylamine 1.) hexane, 1,2-dimethoxyethane; 2.) room temp., 2 h; reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schloegl, Karl; Weissensteiner, Walter
Synthesis, 1982 , # 1 p. 50 - 53
反应条件
1: toluene; POCl3 / 100 °C 2: acetone; palladium/charcoal / Hydrogenation View Scheme
参考文献
Foeldi; Demjen
Chemische Berichte, 1941 , vol. 74, p. 930,933
参考文献
Docken; Spielman
Journal of the American Chemical Society, 1940 , vol. 62, p. 2163
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Foeldi; Demjen
Chemische Berichte, 1941 , vol. 74, p. 930,933
参考文献
Docken; Spielman
Journal of the American Chemical Society, 1940 , vol. 62, p. 2163
反应条件
T=100°C; P=102971 - 110326 Torr; Hydrogenation;
参考文献
Morren
Patent: US2476679 , 1949 ;
参考文献
Wilds; McCormack
Journal of Organic Chemistry, 1949 , vol. 14, p. 45,57
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Kharasch; Kleiman
Journal of the American Chemical Society, 1943 , vol. 65, p. 491
参考文献
Kharasch; Kleiman
Journal of the American Chemical Society, 1943 , vol. 65, p. 491
参考文献
Kharasch; Kleiman
Journal of the American Chemical Society, 1943 , vol. 65, p. 491