2-[4-[(E)-1,2-二苯基丁-1-烯基]苯氧基]-N,N-二甲基-乙胺合成路线 （共 46 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) 1.) hexane, toluene, 90 deg C, 24 h, 2.) THF, reflux, 24 h; Yield given. Multistep reaction;
参考文献
Synthesis, , vol. No. 9, p. 816 - 817
反应条件
1: 1.) Mg / 1.) ether, 2.) reflux, 3 h, ether 2: pyridine hydrochloride / 3.5 h / 220 °C 3: 1.) NaH / 1.) DMF, 2.) 60 deg C, 30 min View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 1342 - 1388
反应条件
1: 1.) Mg / 1.) ether, 2.) reflux, 3 h, ether 2: pyridine hydrochloride / 3.5 h / 220 °C 3: 1.) NaH / 1.) DMF, 2.) 60 deg C, 30 min View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 1342 - 1388
反应条件
1: 94 percent / (CF3CO)2O / 3.2 h / 22 - 30 °C 2: 1.) Mg / 1.) ether, 2.) reflux, 3 h, ether 3: pyridine hydrochloride / 3.5 h / 220 °C 4: 1.) NaH / 1.) DMF, 2.) 60 deg C, 30 min View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 1342 - 1388
反应条件
sodium methylate; hydrogen cation Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 17, # 10 p. 1247 - 1252
反应条件
trifluorormethanesulfonic acid in dichloromethane T=0°C; 3 h;
参考文献
Shiina, Isamu; Sano, Yoshiyuki; Nakata, Kenya; Suzuki, Masahiko; Yokoyama, Toshikazu; Sasaki, Akane; Orikasa, Tomoko; Miyamoto, Tomomi; Ikekita, Masahiko; Nagahara, Yukitoshi; Hasome, Yoshimune
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 24 p. 7599 - 7617
