反应条件
carbon monoxide in tetrahydrofuran byproducts: (C6H5)3P; (Ar), to nickel complex added THF previously saturated with CO, CO passed in for 2.5 h at -20°C, pptd.; ppt. after washing (THF, pentane) obtained (Ph3P)2NiBr2, filtrate evaptd., washed (pentane) extracted (ether), chromy (Al2O3, benzene/petroleumether 1:1), elem. anal., IR;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, p. 1584 - 1585
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1919 - 1920