N,N,2,4,6-五甲基苯胺合成路线 (共 13 条)
反应条件
sodium tetrahydroborate; sulfuric acid in tetrahydrofuran T=10 - 30°C;
参考文献
Synthesis, , # 9 p. 743 - 746
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Synthetic Communications, , vol. 40, # 20 p. 3078 - 3083
反应条件
Ru(Triphos)(TMM); hydrogen; bis-(trifluoromethylsulphonyl)amine in tetrahydrofuran T=150°C; P=60006 Torr; 15 h; AutoclaveInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 36 p. 9554 - 9557
Angew. Chem., , vol. 125, # 36 p. 9733 - 9736
参考文献
Chemische Berichte, , vol. 5, p. 707
Chemische Berichte, , vol. 10, p. 1585 Anm. 1
反应条件
hydrogenchloride; amalgamated zinc; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 63, p. 972
参考文献
Chemische Berichte, , vol. 39, p. 4287
参考文献
Journal of the American Chemical Society, , vol. 63, p. 972
参考文献
Hey
Journal of the Chemical Society, 1931 , p. 1581,1589, 1591
参考文献
Journal of the Chemical Society, , p. 1581,1589, 1591
反应条件
1: aqueous hydrochloric acid; sodium nitrite 2: tin (II)-chloride; aqueous hydrochloric acid View Scheme
参考文献
Emerson
Journal of the American Chemical Society, 1941 , vol. 63, p. 2023