反应条件
1: 1.) BuLi / 1) diethyl ether, 0 deg C, 45 min, room temperature, 30 min; 2) diethyl ether, 0 deg C, 15 min, reflux, 1 h
2: 1.14 g / MnO2 / benzene / 3 h / Heating
3: 0.64 g / aq. HCl / 36 h / Heating
View Scheme
参考文献
Cornforth, John; Cornforth, R. H.; Gray, Robin T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2289 - 2298