5-羟基间苯二甲酸二甲酯合成路线 （共 49 条）
反应条件
thionyl chloride Heating;
参考文献
Wilson, Andrew J.; Hong, Jason; Fletcher, Steven; Hamilton, Andrew D.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 2 p. 276 - 285
参考文献
CLARIANT INTERNATIONAL LTD
Patent: WO2005/118562 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
tetraethylammonium hydroxide in 1,4-dioxane T=20°C; 1 h;
参考文献
Ohgiya, Tadaaki; Nishiyama, Shigeru
Tetrahedron Letters, 2004 , vol. 45, # 33 p. 6317 - 6320
反应条件
in methanol; ethyl acetate; toluene
参考文献
Microcide Pharmaceuticals, Inc.; DAIICHI PHARMACEUTICAL CO., LTD.
Patent: EP1227084 A1, 2002 ;
反应条件
in methanol; hexane; ethyl acetate; toluene
参考文献
Microcide Pharmaceuticals, Inc.; DAIICHI PHARMACEUTICAL CO., LTD.
Patent: EP1227084 A1, 2002 ;
反应条件
potassium hydrogencarbonate in N,N-dimethyl-formamide T=40°C;
参考文献
Guo, Wei; Li, Junfei; Fan, Ningjuan; Wu, Weiwei; Zhou, Peiwen; Xia, Chizhong
Synthetic Communications, 2005 , vol. 35, # 1 p. 145 - 152
反应条件
hydrogenchloride; sodium hydrogencarbonate; triphenylphosphine; trifluoroacetic acid in tetrahydrofuran; dichloromethane; ethyl acetate
反应条件
1: chelidamic acid With thionyl chloride Reflux; 2: methanol T=0 - 20°C; 2 h;
参考文献
Mueller, Sebastian; Sanders, Deborah A.; Di Antonio, Marco; Matsis, Stephanos; Riou, Jean-Francois; Rodriguez, Raphael; Balasubramanian, Shankar
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 32 p. 6537 - 6546
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6851 - 6859
