5-甲基-1,4-己二烯-3-酮合成路线 (共 31 条)
反应条件
palladium on activated charcoal; diethyl ether Hydrogenation;
参考文献
Nasarow; Kuwarsina
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1329
Chem.Abstr., 1949 , p. 2161
反应条件
ethanol; hydrogen sulfide; sodium acetate
参考文献
Nasarow; Kusnetzowa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 122
Chem.Abstr., 1948 , p. 7738
参考文献
Tishchenko,I.G.; Berezovskii,V.V.
Journal of Organic Chemistry USSR (English Translation), 1969 , vol. 5, p. 1735 - 1738
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 1788 - 1792
反应条件
platinum Hydrogenation;
参考文献
Nasarow; Kuwarsina
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1329
Chem.Abstr., 1949 , p. 2161
参考文献
Jelisarowa; Nasarow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1940 , p. 223
Chem.Abstr., 1942 , p. 748
Chem. Zentralbl., 1942 , vol. 113, # I p. 740
Full Text Show Details
Nasarow; Kuwarsina
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 1329
Chem.Abstr., 1949 , p. 2161
反应条件
sulfuric acid; mercuric sulphate in water T=100°C; 4 h;
参考文献
Bioorganic and medicinal chemistry, , vol. 10, # 10 p. 3197 - 3212
反应条件
1: With hydrogenchloride; anhydrous diethylamine hydrochloride; hydroquinone in water
T=100°C; 2 h;
2: T=150 - 210°C;
参考文献
Austin, Kerrie A. B.; Elsworth, Jon D.; Banwell, Martin G.; Willis, Anthony C.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 4 p. 751 - 754
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in diethyl ether
T=18°C; 24 h;
参考文献
Austin, Kerrie A. B.; Elsworth, Jon D.; Banwell, Martin G.; Willis, Anthony C.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 4 p. 751 - 754
反应条件
(i) Me2NH*HCl, aq. HCl, benzene-1,4-diol, EtOH, (ii) dibutyl phthalate, H2O; Multistep reaction;
参考文献
Volynskii,N.P.; Urin,A.B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 2383 - 2386
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 2504 - 2509
反应条件
aluminium trichloride in dichloromethane
T=0°C;
参考文献
Pillot,J.-P. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 2143 - 2146