3,4-亚甲基二氧基乙酰苯胺合成路线 （共 16 条）
反应条件
triethylamine in dichloromethane T=0°C; 0.5 h;
参考文献
Elban, Mark A.; Sun, Wenyue; Eisenhauer, Brian M.; Gao, Rong; Hecht, Sidney M.
Organic Letters, 2006 , vol. 8, # 16 p. 3513 - 3516
反应条件
sodium hydrogencarbonate in chloroform; water Ambient temperature;
参考文献
Luzzio, Michael J.; Besterman, Jeffrey M.; Emerson, David L.; Evans, Michael G.; Lackey, Karen; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 3 p. 395 - 401
反应条件
acetic anhydride in acetic acid
参考文献
Cai, Xiong; Qian, Changgeng
Patent: US2010/184801 A1, 2010 ;
反应条件
hydrogenchloride; sodium acetate; acetic anhydride in water
参考文献
Takasago International Corporation
Patent: US6228547 B1, 2001 ;
反应条件
1: 2: With sodium hydrogencarbonate in water
参考文献
Cai, Xiong; Qian, Changgeng; Zhai, Haixiao
Patent: US2008/234314 A1, 2008 ;
Location in patent: Page/Page column 59 ;
US 20080234314 A1
反应条件
2,4,6-trichloro-1,3,5-triazine; zinc(II) chloride in acetonitrile Beckmann rearrangement; 2 h; Heating;
参考文献
Furuya, Yoshiro; Ishihara, Kazuaki; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 32 p. 11240 - 11241
反应条件
1: palladium; ethanol / Hydrogenation View Scheme
参考文献
Hoffmann-La Roche Inc.
Patent: US4435406 A1, 1984 ;
参考文献
Euro-Celtique S.A.
Patent: US6465472 B1, 2002 ;
反应条件
Candida antarctica lipase B; acetone-oxime in tert-butyl methyl ether T=20°C; 4 h; Molecular sieve;
参考文献
Lal, Samridhi; Snape, Timothy J.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 80 - 86
参考文献
Perkin,W. H.; Robinson; Thomas
Journal of the Chemical Society, 1909 , vol. 95, p. 1978,1983
Full Text Show Details
Rupe; v. Majewski
Chemische Berichte, 1900 , vol. 33, p. 3405
