4-[[(1,1-二甲基乙基)二苯基甲硅烷基]氧基]-环己酮合成路线 （共 6 条）
反应条件
Oxonereg;; sodium 2-iodobenzenesulfonate in acetonitrile T=70°C; 2 h;
参考文献
Uyanik, Muhammet; Akakura, Matsujiro; Ishihara, Kazuaki
Journal of the American Chemical Society, 2009 , vol. 131, p. 251 - 262
反应条件
1H-imidazole in N,N-dimethyl-formamide 5 h; Ambient temperature;
参考文献
Okamura, William H.; Elnager, Hassan Y.; Ruther, Michael; Dobreff, Susanne
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 600 - 610
反应条件
1: 82 percent / 1 M HCl / 0.75 h / 50 °C 2: 83 percent / imidazole / dimethylformamide / 5 h / Ambient temperature View Scheme
参考文献
Okamura, William H.; Elnager, Hassan Y.; Ruther, Michael; Dobreff, Susanne
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 600 - 610
反应条件
1: 93 percent / NH3, Li / diethyl ether / dry ice bath 2: 82 percent / 1 M HCl / 0.75 h / 50 °C 3: 83 percent / imidazole / dimethylformamide / 5 h / Ambient temperature View Scheme
参考文献
Okamura, William H.; Elnager, Hassan Y.; Ruther, Michael; Dobreff, Susanne
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 600 - 610
反应条件
1: 100 percent / imidazole / dimethylformamide / 4 h / 20 °C 2: 97 percent / aq. HCl / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Majewski, Marek; Mackinnon, John
Canadian Journal of Chemistry, 1994 , vol. 72, # 7 p. 1699 - 1704
反应条件
1: NaBH4 / methanol / 3 h / 0 °C 2: 100 percent / imidazole / dimethylformamide / 4 h / 20 °C 3: 97 percent / aq. HCl / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Majewski, Marek; Mackinnon, John
Canadian Journal of Chemistry, 1994 , vol. 72, # 7 p. 1699 - 1704
