4,4'-二硫烷二基二{5-氨基-1-[2,6-二氯-4-(三氟甲基)苯基]-1H-吡唑-3-甲腈}合成路线 （共 6 条）
反应条件
disulfur dichloride in dichloromethane T=20°C;
参考文献
Zhao, Qiqi; Li, Yongqiang; Xiong, Lixia; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 8 p. 4992 - 4998
反应条件
ammonia in chlorobenzene; acetonitrile
参考文献
Bayer Cropscience SA
Patent: US6620943 B1, 2003 ;
反应条件
sulfur dioxide; sodium formate in N,N-dimethyl-formamide T=60°C; P=9000.7 - 9750.8 Torr; 4 h; other reagent, other perhalogenoalkanes, other disulfide; MechanismProduct distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 24 p. 3371 - 3376
反应条件
sodium formate; sodium hydrogencarbonate in water; N,N-dimethyl-formamide
反应条件
in N-methyl-acetamide; water
反应条件
1: 89 percent / Na2S2O4; Na2HPO4 / dimethylformamide; H2O / 1 h / 20 °C 2: 95 percent / CF3COOH; aq. H2O2 / CH2Cl2 / 4 h / 10 - 12 °C View Scheme
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2006 , vol. 127, # 7 p. 948 - 953
