2,3,4,6-四-O-乙酰基-1,5-脱水-D-甘露醇合成路线 （共 25 条）
反应条件
sodium cyanoborohydride in tert-butyl alcohol 0.666667 h; UV-irradiationInert atmosphere;
参考文献
Tetrahedron, , vol. 69, # 46 p. 9656 - 9662
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1.5 h; Heating;
参考文献
Carbohydrate Research, , vol. 343, # 10-11 p. 1743 - 1753
反应条件
1: 1,5-anhydro-2,3-dideoxy-D-erythro-hex-2-enitol With osmium(VIII) oxide; 4-methylmorpholine N-oxide in water; acetone 2: acetic anhydride With pyridine; 4-(N,N-dimethlyamino)pyridine T=20°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 23 p. 7946 - 7956
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene Heating;
参考文献
Organic Letters, , vol. 5, # 10 p. 1649 - 1652
反应条件
1-thio-2,3,4,6-tetra-O-acetyl-β-D-mannopyranose; t-BuON=NOt-Bu in hexane T=60°C; 2.5 h; Yields of byproduct given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 17 p. 2881 - 2889
反应条件
1: benzylamine / CHCl3 / 1 h / 0 °C 2: 72.3 percent / pyridinium chlorocromate / CH2Cl2 / 24 h / Ambient temperature 3: 51.7 percent / trimethylsilyl trifluoromethanesulfonate / CH2Cl2 / 72 h / -10 °C View Scheme
参考文献
Carbohydrate Research, , vol. 121, p. 175 - 186
反应条件
1: 72.3 percent / pyridinium chlorocromate / CH2Cl2 / 24 h / Ambient temperature 2: 51.7 percent / trimethylsilyl trifluoromethanesulfonate / CH2Cl2 / 72 h / -10 °C View Scheme
参考文献
Carbohydrate Research, , vol. 121, p. 175 - 186
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3175
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol 0.833333 h; Irradiation;
参考文献
Carbohydrate Research, , vol. 337, # 18 p. 1623 - 1632
参考文献
Journal of the American Chemical Society, , vol. 71, p. 140,142
