LiCl; BrCH2CH2Br; (CH3)3SiCl in tetrahydrofuran (N2); drying LiCl for 20 min (150-170°C, 1 mbar), addn. of Zn powder (1.4 equiv.), addn. of THF, activation by Br(CH2)2Br (5 percent), Me3SiCl (1 percent), addn. of C8H17Br at room temp., storage for 24 h; Angew. Chem., Int. Ed., 2006, 45, 6040;

titanium(IV) isopropylate; tert.-butylhydroperoxide in diethyl ether T=-78°C; 12 h;

2-chloro-1,2-diphenyl-ethanone; ((S)-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl)PdCl2*2THF in tetrahydrofuran T=20°C;

benzamide in tetrahydrofuran T=25°C; 0.416667 h;

carbon monoxide; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; P=760.051 Torr; 24 h;

PdCl2(bis(o-diphenylphosphanylphenyl ether)) in N,N-dimethyl-formamide T=23°C; 20 h;