4-(乙氧羰基)苯基碘化锌合成路线 （共 24 条）
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Journal of the American Chemical Society, , vol. 125, # 13 p. 3867 - 3870
反应条件
in tetrahydrofuran 70°C, 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 36 p. 6040 - 6044
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,1'-bis(diphenylphosphino)ferrocene; Ph–ZnI in tetrahydrofuran T=40°C; Negishi coupling reaction; 1 h; Inert atmosphere;
参考文献
Takahashi, Hideki; Inagaki, Shinya; Yoshii, Naoko; Gao, Fuxing; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2794 - 2797
反应条件
1: 4-ethoxycarbonylphenylzinc iodide With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 5 h; 2: 1,4-Diiodobenzene With N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0) in various solvent(s) T=45°C; 10 h; 3: With iodine in various solvent(s)
参考文献
Hossain, Kabir M.; Kameyama, Toru; Shibata, Takanori; Takagi, Kentaro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2415 - 2420
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 T=80°C; Substitution; 24 h;
参考文献
Hossain, Kabir M.; Takagi, Kentaro
Chemistry Letters, 1999 , # 11 p. 1241 - 1242
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; 1-iodo-n-heptane; N,N,N',N'-tetramethyl-urea; [RhCl(η2:η2-cycloocta-1,5-diene)]2 T=40°C; 24 h;
参考文献
Takahashi, Hideki; Inagaki, Shinya; Nishihara, Yasushi; Shibata, Takanori; Takagi, Kentaro
Organic Letters, 2006 , vol. 8, # 14 p. 3037 - 3040
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 T=80°C; Substitution; 24 h;
参考文献
Hossain, Kabir M.; Takagi, Kentaro
Chemistry Letters, 1999 , # 11 p. 1241 - 1242
反应条件
1: carbon monoxide With 1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=20°C; P=760.051 Torr; 0.166667 h; 2: 4-ethoxycarbonylphenylzinc iodide With ethylene dibromide in tetrahydrofuran T=60°C; 3 h;
参考文献
Kobayashi, Kana; Nishimura, Yugo; Gao, Fuxing; Gotoh, Kazuma; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1949 - 1952
反应条件
Ni(Cl){2-(Ph2P)C6H4NCH(Ph)P(O)Ph2} in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=70°C; Negishi coupling reaction; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Li; Wang, Zhong-Xia
Chemical Communications, 2011 , vol. 47, # 5 p. 1598 - 1600
