3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1,2-dibromomethane in tetrahydrofuran T=40°C; 1.5 h;
参考文献
US2009/75989 A1, ;
Page/Page column 63-64 ;
US 20090075989 A1
反应条件
magnesium; bromine in diethyl ether
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 50, # 2 p. 321 - 326,258 - 263
反应条件
magnesium in tetrahydrofuran; dichloromethane
反应条件
iodine; magnesium in tetrahydrofuran; anhydrous xylene; Sec-butyl alcohol
反应条件
1: diethyl ether 2: potassium hydrogen sulfate / 160 °C View Scheme
参考文献
Ziering et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 894,897, 9O2
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=-30°C; 0.166667 h;
参考文献
Boully, Ludovic; Darabantu, Mircea; Turck, Alain; Ple, Nelly
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 7 p. 1423 - 1428
参考文献
Baddar et al.
Journal of the Chemical Society, 1957 , p. 1690,1699
反应条件
in tetrahydrofuran T=0°C;
参考文献
Ngu, Khehyong; Weinstein, David S.; Liu, Wen; Langevine, Charles; Combs, Donald W.; Zhuang, Shaobin; Chen, Xing; Madsen, Cort S.; Harper, Timothy W.; Ahmad, Saleem; Robl, Jeffrey A.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 14 p. 4141 - 4145
反应条件
1: PdCl2 / tetrahydrofuran 2: acetic acid, hydrobromic acid View Scheme
参考文献
Takatsu; Takeuchi; Sato
Molecular crystals and liquid crystals, 1984 , vol. 108, # 1-2 p. 157 - 164
