3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
1: in tetrahydrofuran T=0°C; Grignard reaction; 3.5 h; Inert atmosphere; 2: With potassium hydroxide in methanol 24 h; Reflux;
参考文献
Fleischer, Ivana; Pfaltz, Andreas
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 95 - 99
反应条件
(1,2,3,4,5-pentamethyl-cyclopenta-2,4-dienylmethyl)PPh2; nickel dichloride in diethyl ether T=25°C; 3 h;
参考文献
Uemura, Minoru; Yorimitsu, Hideki; Oshima, Koichiro
Chemical Communications, 2006 , # 45 p. 4726 - 4728
反应条件
iron(III) chloride; potassium carbonate in tetrahydrofuran; diethyl ether T=10 - 15°C; 18 h;
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
反应条件
diethyl ether; benzene
参考文献
Journal of the American Chemical Society, , vol. 66, p. 415
反应条件
1: in tetrahydrofuran T=-78 - -20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=-20 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Gaggero; Albanese
Tetrahedron, 2012 , vol. 68, # 35 p. 7129 - 7132
参考文献
Funaki, Kenji; Kawai, Hiroshi; Sato, Tetsuo; Oi, Shuichi
Chemistry Letters, 2011 , vol. 40, # 9 p. 1050 - 1052
反应条件
diethyl ether; hydrogen; phosphorus trichoride
参考文献
Mann; Chaplin
Journal of the Chemical Society, 1937 , p. 527,530
反应条件
bismuth(III) chloride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 48, p. 516
反应条件
1: diethyl ether 2: PBr3 3: ethyl-butyl ether; copper-powder 4: AlI3 / 120 °C View Scheme
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 111,117
反应条件
1: in tetrahydrofuran; diethyl ether T=-78 - 20°C; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether; water
参考文献
BANYU PHARMACEUTICAL CO., LTD.
Patent: EP1719756 A1, 2006 ;
Location in patent: Page/Page column 49 ;
EP 1719756 A1
