3-甲基-CBS-氧硼啶合成路线 (共 731 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; Kumada Cross-Coupling; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Synthesis (Germany), , vol. 45, # 19 art. no. SS-2013-T0413-OP, p. 2752 - 2762
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
1: 1-n-heptyne With isopropylmagnesium chloride in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: 4-methoxyphenyl magnesium bromide With oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-5 - 0°C; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
oxygen in tetrahydrofuran T=20°C; 0.75 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 45 p. 13788 - 13789
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=-20°C; 1 h; Inert atmosphere; chemoselective reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 24 h; Heating;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran Kumada-Corriu reaction; 48 h; Heating;
参考文献
Tetrahedron, , vol. 63, # 20 p. 4304 - 4309