3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=20°C; 18 h;
参考文献
Filosa, Rosanna; Peduto, Antonella; de Caprariis, Paolo; Saturnino, Carmela; Festa, Michela; Petrella, Antonello; Pau, Amedeo; Pinna, Gerard Aime; La Colla, Paolo; Busonera, Bernardetta; Loddo, Roberta
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 3 p. 293 - 306
反应条件
in tetrahydrofuran
T=0°C; 1 h; Schlenk technique;
参考文献
Tan, Boon-Hong; Dong, Jinghua; Yoshikai, Naohiko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 38 p. 9610 - 9614
反应条件
1: diethyl ether / 2 h / Heating
2: H2SO4, AcOH / 0.33 h / Heating
View Scheme
参考文献
Schneider, Martin R.; Angerer, Erwin von; Schoenenberger, Helmut; Michel, Ralf Th.; Fortmeyer, H. P.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1070 - 1077
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran
Kumada-Corriu reaction; 24 h; Heating;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
参考文献
Baciocchi, Enrico; Bietti, Massimo; Putignani, Lorenza; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5952 - 5960
反应条件
tris-(dibenzylideneacetone)dipalladium(0); zinc(II) chloride; lithium iodide in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8)
T=55°C; P=2660.18 Torr; 5 h; Inert atmosphereAutoclave;
参考文献
Ohashi, Masato; Kambara, Tadashi; Hatanaka, Tsubasa; Saijo, Hiroki; Doi, Ryohei; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3256 - 3259
反应条件
in tetrahydrofuran
T=20°C; 20 h;
参考文献
Alphonse, France-Aimee; Suzenet, Franck; Keromnes, Anne; Lebret, Bruno; Guillaumet, Gerald
Synthesis, 2004 , # 17 p. 2893 - 2899
反应条件
FeCl(THF)L1 in diethyl ether; dichloromethane
T=20°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Chard, Elliott F.; Dawe, Louise N.; Kozak, Christopher M.
Journal of Organometallic Chemistry, 2013 , vol. 737, p. 32 - 39
反应条件
1: benzyl alcohol With n-butyllithium; chloro-diphenylphosphine in tetrahydrofuran
2: With methyl iodide in tetrahydrofuran
T=20°C; 1 h;
3: 4-methoxyphenyl magnesium bromide in tetrahydrofuran
T=20°C; 1 h;
参考文献
Shintou, Taichi; Kikuchi, Wataru; Mukaiyama, Teruaki
Chemistry Letters, 2003 , vol. 32, # 8 p. 676 - 677
反应条件
C4H6Cl2N2Ni; C33H27NP2 in tetrahydrofuran
T=20°C; Kumada-Corriu reaction; 8 h; Inert atmosphere;
参考文献
Ghosh, Raju; Sarkar, Amitabha
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8283 - 8286
