3-甲基-CBS-氧硼啶合成路线 （共 731 条）
反应条件
iron(III) chloride amine-bis(phenolate) complex in diethyl ether; dichloromethane
0.5 h;
参考文献
Chowdhury, Rajoshree Roy; Crane, Angela K.; Fowler, Candace; Kwong, Philip; Kozak, Christopher M.
Chemical Communications, 2008 , # 1 p. 94 - 96
反应条件
diethyl ether
Dehydratisierung des nach der Hydrolyse erhaltenen Reaktionsprodukts;
参考文献
Mentzer; Dat Xuong
Bulletin de la Societe Chimique de France, 1947 , p. 885,891
反应条件
iron (III) acetylacetonate in diethyl ether
Inert atmosphere; Kinetics; Time;
参考文献
Hedstroem, Anna; Bollmann, Ulla; Bravidor, Jenny; Norrby, Per-Ola
Chemistry - A European Journal, 2011 , vol. 17, # 43 p. 11991 - 11993
反应条件
diethyl ether
anschliessend Behandeln mit wss. Schwefelsaeure;
参考文献
Rubin; Wishinsky
Journal of the American Chemical Society, 1946 , vol. 68, p. 338
参考文献
Rubin; Wishinsky
Journal of the American Chemical Society, 1946 , vol. 68, p. 338
反应条件
in not given
N2; cooling a flask with aryl-Grignard reagent to -78°C, addn. ofsolid Sn compd. (0.5 equiv.), stirring at -78°C for 20 min, warm ing to room temp., stirring over several hs.; removal of volatiles under reduced pressure, addn. of hexanes, filtration (Celite), washing the solid with hexanes, concg. the combined organic soln., standing until the oil is solidified;
参考文献
Thomas, J. Christopher; Peters, Jonas C.
Inorganic Chemistry, 2003 , vol. 42, # 17 p. 5055 - 5073
参考文献
Yagupol'skii,L.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 1920 - 1925
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 9 p. 1967 - 1973
反应条件
(i) THF, (ii) /BRN= 114632/; Multistep reaction;
参考文献
Ramadas,S.R.; Srinivasan,P.S.
Journal fuer Praktische Chemie (Leipzig), 1977 , vol. 319, p. 169 - 173
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 2 p. 505 - 509
反应条件
Erhitzen des Reaktionsprodukts mit Aethylendiamin;
参考文献
Hill; Johnston
Journal of the American Chemical Society, 1954 , vol. 76, p. 920
