反应条件
2-picoline in further solvent(s)
byproducts: (HNC6H8)Cl; passing dry H2S in a soln. of PCl3 in 2-methylpyridine, exotherm react., cooling of mixture in H2O-bath to 20-30°C, yellow ppt.; condensation of excess 2-methylpyridine, elution of residue with CS2 (twice), isolation of P4S3 by sepn. of solvent from eluate, washing with CH2Cl2, drying in vac.; dissoln. of solid residue in CH3CN and isolation as Ph4P-salt; elem. anal.;
参考文献
Fluck, E.; Neumueller, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1986 , vol. 534, p. 27 - 30
