131543-46-9合成路线 （共 480 条）
参考文献
Hollstein, Ulrich; Krisov, Galen E.
Organic Magnetic Resonance, 1980 , vol. 14, # 4 p. 300 - 304
反应条件
ethanol T=80 - 90°C; Produkt: Traubensaeurenitril;
参考文献
Strecker
Zeitschrift fuer Chemie, 1868 , p. 216
参考文献
Societe Francaise Hoechst
Patent: US5550250 A1, 1996 ;
反应条件
in ethanol; water T=70°C; 16 h;
参考文献
Farfan, Norberto; Cuellar, Laura; Aceves, Juan Manuel; Contreras, Rosalinda
Synthesis, 1987 , # 10 p. 927 - 929
反应条件
sodium hydrogensulfite 1.) H2O, 70 deg C, 2.) 70 deg C -> RT, 15 min; Multistep reaction;
参考文献
Hollstein, Ulrich; Krisov, Galen E.
Organic Magnetic Resonance, 1980 , vol. 14, # 4 p. 300 - 304
反应条件
1: formaldehyd; ethylamine in water T=31°C; Cooling with ice; 2: methylamine in water T=3 - 5°C; Cooling with ice; 3: ethane-1,2-dial; acetic acid Product distribution / selectivity;
参考文献
US2010/249432 A1, ;
Page/Page column 5 ;
参考文献
Martinez-Bernhardt, Rolando; Castro, Peter P.; Godjoian, Gayane; Gutierrez, Carlos G.
Tetrahedron, 1998 , vol. 54, # 31 p. 8919 - 8932
反应条件
ammonium acetate; acetic acid 2 h; Reflux;
参考文献
Taile; Hatzade; Gaidhane; Ingle
Journal of Heterocyclic Chemistry, 2010 , vol. 47, # 4 p. 903 - 907
反应条件
magnesium sulfate; acetic acid in acetic acid n-butyl ester 4 h; Heating;
参考文献
Iwata, Satoru; Namekata, Junji; Tanaka, Kiyoshi; Mitsuhashi, Keiryo
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 8 p. 1971 - 1976
反应条件
sodium hydrogensulfite 1.) H2O, 70 deg C, 2.) 70 deg C -> RT, 15 min; Multistep reaction;
参考文献
Hollstein, Ulrich; Krisov, Galen E.
Organic Magnetic Resonance, 1980 , vol. 14, # 4 p. 300 - 304
