131543-46-9合成路线 (共 480 条)
反应条件
hydrogenchloride; 15NH4Cl in water
T=95°C; 1.5 h;
参考文献
Alia; Matysik; Erkelens; Hulsbergen; Gast; Lugtenburg; De Groot
Chemical Physics Letters, 2000 , vol. 330, # 3-4 p. 325 - 330
反应条件
in ethanol; water; ethyl acetate; N,N-dimethyl-formamide
参考文献
Mao, Fei; Heller, Adam
Patent: US2003/96997 A1, 2003 ;
参考文献
Kuhn; Drawert
Justus Liebigs Annalen der Chemie, 1954 , vol. 590, p. 55,61
反应条件
in methanol; water
7 h; Heating;
参考文献
Feliciano, Arturo San; Caballero, Esther; Pereira, Juan A. P.; Puebla, Pilar
Tetrahedron, 1989 , vol. 45, # 20 p. 6553 - 6562
反应条件
1: formaldehyd; ethylamine in water
0.5 h; Cooling with ice;
2: ethane-1,2-dial; acetic acid; methylamine in water
T=0 - 20°C; 36 h;
3: With sulfur
24 h;
参考文献
Rodriguez, Hector; Gurau, Gabriela; Holbrey, John D.; Rogers, Robin D.
Chemical Communications, 2011 , vol. 47, # 11 p. 3222 - 3224
反应条件
acetic acid
Heating;
参考文献
Chioccara,F. et al.
Journal of the Chemical Society, Chemical Communications, 1977 , p. 863 - 864
反应条件
sodium hydroxide in methanol; water
参考文献
Sato, Nobuhiro
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 149 - 152
参考文献
Donciu
Monatshefte fuer Chemie, 1895 , vol. 16, p. 8,12
反应条件
Title compound not separated from byproducts;
参考文献
Castro, Peter P.; Tihomirov, Serge; Gutierrez, Carlos G.
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 5179 - 5181
反应条件
Glyoxalsulfat reagiert analog;
参考文献
Faass; Hilgert
Chemische Berichte, 1954 , vol. 87, p. 1343,1350
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Furberg; Hassel
Acta Chemica Scandinavica (1947-1973), 1950 , vol. 4, p. 1584
Full Text Show Details
Fuchs et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1972 , p. 357