(三甲基硅基)甲基氯化镁合成路线 (共 130 条)
参考文献
Tamao,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1958 - 1969
参考文献
Tamao,K. et al.
Chemistry Letters, 1976 , p. 1239 - 1242
反应条件
1: in tetrahydrofuran
T=-5°C; 0.5 h;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran
T=20°C; 2 h;
参考文献
Kuethe, Jeffrey T.; Wong, Audrey; Davies, Ian W.
Organic Letters, 2003 , vol. 5, # 21 p. 3975 - 3978
反应条件
nickel dichloride in tetrahydrofuran
Kumada coupling reaction;
参考文献
Delgado, Rieardo; Blakey, Simon B.
European Journal of Organic Chemistry, 2009 , # 10 p. 1506 - 1510
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
16 h; Heating;
参考文献
Ni, Zhi-Jie; Luh, Tien-Yau
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 2129 - 2131
反应条件
(i) Et2O, dioxane, (ii) (heating); Multistep reaction;
参考文献
Francos, Javier; Zaragoza-Calero, Silvia; O'Hara, Charles T.
Dalton Transactions, 2014 , vol. 43, # 3 p. 1408 - 1412
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=25 - 35°C; 18 h;
参考文献
Andreini, Bianca Patrizia; Carpita, Adriano; Rossi, Renzo; Scamuzzi, Barbara
Tetrahedron, 1989 , vol. 45, # 17 p. 5621 - 5640
反应条件
NiCl2((PPh3)P)2 in ethylene glycol dimethyl ether; diethyl ether
1.5 h; Heating;
参考文献
Hevesi, Laszlo; Hermans, Bernard; Allard, Christophe
Tetrahedron Letters, 1994 , vol. 35, # 36 p. 6729 - 6730
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II)
参考文献
Hayashi, Tamio; Kabeta, Keiji; Hamachi,Itaru; Kumada, Makoto
Tetrahedron Letters, 1983 , vol. 24, # 28 p. 2865 - 2868
反应条件
anschliessend mit Wasser;
参考文献
Speier; Daubert
Journal of the American Chemical Society, 1948 , vol. 70, p. 1400