(三甲基硅基)甲基氯化镁合成路线 （共 130 条）
反应条件
sulfuric acid
1.) THF, 0 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Hwu, Jih Ru; Gilbert, Bryant A.
Journal of the American Chemical Society, 1991 , vol. 113, # 15 p. 5917 - 5918
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
15 h; Ambient temperature;
参考文献
Hayashi, Tamio; Fujiwa, Takaaki; Okamoto, Yasuo; Katsuro, Yoshio; Kumada, Makoto
Synthesis, 1981 , # 12 p. 1001 - 1003
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
lithium
1.) diethyl ether/ THF, -78 deg C, 3 h, 2.) room temperature; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Fernandez-Simon, Jose L.; Concellon, Jose M.; Yus, Miguel
Tetrahedron Letters, 1989 , vol. 30, # 43 p. 5927 - 5928
反应条件
CoCl2 in tetrahydrofuran
T=25°C; 14 h;
参考文献
Affo, Walter; Ohmiya, Hirohisa; Fujioka, Takuma; Ikeda, Yousuke; Nakamura, Tomoaki; Yorimitsu, Hideki; Oshima, Koichiro; Imamura, Yuki; Mizuta, Tsutomu; Miyoshi, Katsuhiko
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 8068 - 8077
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
NiCl2((PPh3)P)2 in ethylene glycol dimethyl ether; diethyl ether
4.5 h; Heating;
参考文献
Hevesi, Laszlo; Hermans, Bernard; Allard, Christophe
Tetrahedron Letters, 1994 , vol. 35, # 36 p. 6729 - 6730
反应条件
in diethyl ether
41 h; Heating;
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 251 - 255
反应条件
niobium bromide in diethyl ether
15 h; Ambient temperaturecatalytic activity of several transition metal complexes; Product distribution;
参考文献
Hayashi, Tamio; Fujiwa, Takaaki; Okamoto, Yasuo; Katsuro, Yoshio; Kumada, Makoto
Synthesis, 1981 , # 12 p. 1001 - 1003
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
16 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ni, Zhi-Jie; Luh, Tien-Yau
Journal of the Chemical Society, Chemical Communications, 1988 , # 15 p. 1011 - 1012
