1-氟-1,1-二硝基乙烷合成路线 （共 6 条）
反应条件
fluorspar; fluorine T=-60 - -55°C;
参考文献
Fokin, A. V.; Radchenko, V. P.; Galakhov, V. S.; Stolyarov, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1202 - 1204
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1349 - 1351
反应条件
XeF2; water; sodium carbonate in dichloromethane 0.5 h; Ambient temperature;
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Varyagina, L. G.; Trubitsin, A. E.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 12 p. 2276 - 2279
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 12 p. 2490 - 2493
反应条件
NAF; antimony(V) pentachloride in dichloromethane T=20°C; 1 h; other solvent: CH3CN; other reagents: HCl, (CH3)4NCl; Product distribution;
参考文献
Erashko, V. I.; Baryshnikov, A. T.; Zubanova, N. I.; Tishaninova, A. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 2 p. 1939 - 1944
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 9, p. 2106 - 2111
反应条件
perchloryl fluoride in methanol; water
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Trubitsin, A. E.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 2.1 p. 228 - 231
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 2 p. 272 - 276
反应条件
XeF2; dichloromethane T=15 - 20°C;
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Trubitsin, A. E.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 8 p. 1485 - 1487
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 8 p. 1657 - 1659
反应条件
XeF2; dichloromethane; water; dinitrogen tetraoxide 8 h; Ambient temperatureother time, other concentration, other additions; Product distributionMechanism;
参考文献
Tselinskii, I. V.; Mel'nikov, A. A.; Varyagina, L. G.; Trubitsin, A. E.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 12 p. 2276 - 2279
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 12 p. 2490 - 2493
