4-羟基-7-甲基-1,8-萘啶-3-羧酸乙酯合成路线 (共 11 条)
反应条件
in diphenylether 0.5 h; Heating;
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
参考文献
American Cyanamid Company
Patent: US6228869 B1, 2001 ;
US 6228869 B1
反应条件
1: 90 percent / ethanol / 16 h / Heating 2: 71 percent / diphenyl ether / 0.5 h / Heating View Scheme
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
反应条件
1: 90 percent / ethanol / 16 h / Heating 2: 71 percent / diphenyl ether / 0.5 h / Heating View Scheme
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
反应条件
1: 72 percent / K2CO3 / dimethylformamide / 90 - 100 °C 2: 91 percent / aq. NaOH / tetrahydrofuran / 8 h / Heating View Scheme
参考文献
Synthesis, , # 14 art. no. P04405SS, p. 2315 - 2320
反应条件
1: 4.7 g / SeO2 / H2O; pyridine / 10 h / Heating 2: KOH / H2O / 1.75 h / 100 °C 3: 4.0 g / quinoline / 8 h / Heating 4: 3.3 g / phosphoryl bromide / 0.75 h / 140 - 150 °C View Scheme
参考文献
Barlin, Gordon B.; Tan, Weng-Lai
Australian Journal of Chemistry, 1984 , vol. 37, # 5 p. 1065 - 1073
反应条件
potassium hydroxide in water 1.75 h;
参考文献
Barlin, Gordon B.; Tan, Weng-Lai
Australian Journal of Chemistry, 1984 , vol. 37, # 5 p. 1065 - 1073
反应条件
potassium carbonate in N,N-dimethyl-formamide T=90 - 100°C;
参考文献
Singh, Ram; Geetanjali
Synthesis, 2005 , # 14 art. no. P04405SS, p. 2315 - 2320
参考文献
Beecham Group Limited
Patent: US4166817 A1, 1979 ;
反应条件
ammonium hydroxide; trichlorophosphate
参考文献
Sumitomo Chemical Company, Limited
Patent: US3963736 A1, 1976 ;